Synthesis and thermal characterization of composites based on Epidian 601 with flame retardants compounds
Artykuł w czasopiśmie
MNiSW
140
Lista 2023
| Status: | |
| Autorzy: | Wnuczek Krystyna, Sowa Krolina , Podkościelna Beata, Klepka Tomasz |
| Dyscypliny: | |
| Aby zobaczyć szczegóły należy się zalogować. | |
| Rok wydania: | 2023 |
| Wersja dokumentu: | Elektroniczna |
| Język: | angielski |
| Numer czasopisma: | 5 |
| Wolumen/Tom: | 95 |
| Strony: | 1 - 15 |
| Web of Science® Times Cited: | 1 |
| Scopus® Cytowania: | 1 |
| Bazy: | Web of Science | Scopus |
| Efekt badań statutowych | NIE |
| Finansowanie: | The project/research was financed in the framework of the project Lublin University of Technology – Regional Excellence Initiative, funded by the Polish Ministry of Science and Higher Education (contract no. 030/RID/2018/19). |
| Materiał konferencyjny: | NIE |
| Publikacja OA: | NIE |
| Abstrakty: | angielski |
| This study presents the preparation and flammability characteristics of polymeric composites based on the epoxy resin Epidian® 601. The triethylenetetramine (TETA) and commercial curing agents based on polyamines (IDA and PAC) were used as crosslinking compounds. Moreover, two flame retardant compounds were added to this composition, the commercial Fire Retardant (FR) and triphenyl phosphate (TP). The chemical structure of the composites and the course of curing processes were confirmed by the ATR/FT-IR (Attenuated Total Reflection–Fourier Transform Infrared) analysis. The influence of different amounts of FR or TP on the flammability and thermal resistance was discussed in detail. After the flammability test the samples were also studied to assess their thermal destruction. In addition, the composites were subjected to the swelling tests, solvent resistance, and microscopic observations. The DSC curves revealed that all materials were characterized by good thermal properties. All materials were temperature resistant up to 300 °C. Furthermore, the measurements of the hardness of the composite demonstrated that the material EP601 + TETA + 10 %FR is the hardest. The addition of FR and RP influenced the flammability of the composites increasing the thermal resistance. The ageing tests in methanol, acetone, hydrochloric acid, and potassium hydroxide were also carried out. |
