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The paper presents issues regarding self-healing isophorone diisocyanate (IPDI) microcap-
sules applied in fiber metal laminates (FMLs) based on magnesium AZ31 and a carbon-reinforced
polymer composite. The aim of this work is to analyze the morphology of the produced PU/PUa
microcapsules containing IPDI and their behavior in a self-healing layer in FMLs. By means of SEM, it
was confirmed that the microcapsules (MCs) had a narrow size distribution. Therefore, the developed
MCs, having sizes ranging from 10 to 35 μm, might contribute to an improved self-healing coating,
which benefits from the advantages of both small and larger-sized MCs. The positive result of the
work is that there is a possibility to improve the properties of FMLs with added MCs, i.e., in corrosion
and mechanical phenomena.